A detailed analysis of the microstructure of layered semiconductor het
erostructures is only possible if the interface between the various la
yers can be accurately located. Microstructural features whose charact
erisation is dependent on the location of the interface include the pl
anarity and width of the layers, the composition profile and the geome
try of misfit dislocations (in the particular case of lattice mismatch
ed heterostructures). We report on an investigation to image, at high
resolution in the transmission electron microscope, the interface in a
n In0.2Ga0.8As/GaAs structure grown by molecular beam epitaxy. The dif
ficulty in locating the interface, due to similarity in electron optic
al behaviour of GaAs and In0.2Ga0.8As when imaged in a [110] direction
, was overcome by incorporating into the structure a ''marker layer''
of AlAs two unit cells thick (11.4 angstrom in total) between the GaAs
and the In0.2Ga0.8As layers. Lattice fringe images of an In0.2Ga0.8As
/AlAs/GaAs structure are presented which show, at near atomic resoluti
on, the location of the misfit dislocations relative to the In0.2Ga0.8
As/GaAs interface.