X. Chaudot et al., COMPARISON OF SUPERCRITICAL-FLUID EXTRACTION WITH SOLVENT SONICATION FOR CHEMICAL WARFARE AGENT DETERMINATION IN ALKYD PAINTED PLATES, HRC. Journal of high resolution chromatography, 21(8), 1998, pp. 457-463
Supercritical fluid extraction (SFE) of alkyl alkylphosphonofluoridate
s and dialkyl alkylphosphonates from painted plates was investigated.
It was found that SFE recoveries compared favorably with conventional
solvent sonication results. Stability studies of the samples were carr
ied out over a period of two months. This investigation showed that th
e concentration of phosphonofluoridates decreased over a long period.