Cy. Nakakura et al., A HIGH-SPEED VARIABLE-TEMPERATURE ULTRAHIGH-VACUUM SCANNING TUNNELINGMICROSCOPE, Review of scientific instruments, 69(9), 1998, pp. 3251-3258
An ultrahigh vacuum scanning tunneling microscopy (STM)system capable
of collecting constant-current STM images at rates exceeding 1 image/s
at temperatures up to 900 K was designed, built, and tested. The micr
oscope uses an inchworm to push a scanner assembly through a quartz tu
be towards the sample. When the scanner is within tunneling range of t
he surface, the inchworm is decoupled from the scanner, resulting in a
small, rigid mechanical loop with a high resonant frequency. The cyli
ndrical symmetry and the use of low thermal expansion materials reduce
s image distortion due to thermal drift. An analog proportional-integr
al controller with tilt correction is used to maintain a constant tunn
el current. A personal computer running Microsoft WINDOWS '95 is used
to control all other instrument functions, as well as for data acquisi
tion, manipulation, and storage. Problems associated with the non real
time nature of the operating system were overcome by collecting the S
TM images within a virtual device driver. By taking advantage of the W
INDOWS '95 multimedia functions, the time required to display and save
images was reduced below 5 ms using a standard personal computer with
no special hardware other than data acquisition cards. Sample STM ima
ges of Pd(111) and halogens adsorbed on Cu(100) are presented. (C) 199
8 American Institute of Physics. [S0034-6748(98)02209-6].