Cj. Passo et al., PERFORMANCE OF THE PACKARD TRI-CARB(R) 2770TR SL LIQUID SCINTILLATIONANALYZER FOR C-14 DATING/, Radiocarbon, 40(1), 1998, pp. 193-200
We present results that demonstrate the potential of the Packard Tri-C
arb(R) Model 2770TR/SL for radiocarbon dating. For 2 g of sample benze
ne, a stable background count rate of 0.307 cpm and a stable counting
efficiency of 64.78% were determined using a 13-75 keV counting window
. Changes to the mathematical routines for t-SIE (quench indicating pa
rameter) calculation and a reduction in the activity of the external s
tandard have enabled stability of the t-SIE to be achieved, and combin
ed with the use of a suitable balance point counting window; all of th
ese factors give the stability of performance required for C-14 dating
. Calculations based on the above parameters indicate that the limit o
f detection for 2 g samples, counted for 5000 min, is >48,900 yr sp. T
he great advantage of this system is that these data were acquired usi
ng inexpensive standard 7-mL low potassium borosilicate glass vials. V
ial holders manufactured from BGO reduced the background to 0.15 cpm w
ith a minimum effect on efficiency (64.46% for 13-75 keV). A similar c
alculation of the limit of detection gave >51,700 sp. The use of the B
GO vial holders in other instruments employing time-resolved liquid sc
intillation counting (TR-LSC) (Models 2250CA and 2260XL) also brought
about significant improvements in detection limits.