The influence of microstructure on the indentation cracking behavior o
f molybdenum disilicide (MoSi2) has been examined. The indentation res
ponse of samples produced by various methods has been measured to exam
ine the elastic/plastic nature, hardness, and fracture toughness. Frac
ture toughness comparisons were made by measuring indentation crack le
ngths, observing the elastic/plastic indentation response, and quantif
ying the differences in the indentation cracking behavior. Further inf
ormation was gained by monitoring the acoustic activity during indenta
tion for selected specimens. It has been observed that the fine grain
size and the dispersion of the silica phase promote microcracking and
crack deflection.