The synthesis of nanosized zinc blende using organic surfactants as an
organic template results in a narrow textural mesopore size distribut
ion after surfactant removal. The findings from X-ray diffraction meas
urements indicate randomly ordered pores, which is in goad agreement w
ith the reported results of transmission electron microscopy investiga
tions. The complete removal of surfactants-much more difficult for mic
roporous sulfides than for microporous oxides-is confirmed by Fourier
transform infrared spectroscopy.