We present direct evidence of dynamical diffraction of x rays from a q
uasicrystal. High-resolution x-ray-diffraction measurements of the Al-
Pd-Mn face-centered icosahedral quasicrystal were performed, revealing
a mosaic full width at half maximum of less than 0.001-degrees. In a
second experiment, the anomalous transmission of x rays (the Borrmann
effect) was observed. These measurements show that nearly perfect quas
icrystals may be grown to centimeter-size dimensions allowing x-ray te
chniques based upon dynamical diffraction to be brought to bear on the
analysis of icosahedral structures.