APPLICATION OF TLC FOR DETERMINATION OF HIGH EXPLOSIVE RESIDUES IN WATER AND SOIL SAMPLES

Authors
BLADEK J PAPLINSKI A NEFFE S ROSTKOWSKI A
Citation
J. Bladek et al., APPLICATION OF TLC FOR DETERMINATION OF HIGH EXPLOSIVE RESIDUES IN WATER AND SOIL SAMPLES, Chemia Analityczna, 43(4), 1998, pp. 711-718
Citations number
12
Categorie Soggetti
Chemistry Analytical
Journal title
Chemia Analityczna → ACNP
ISSN journal
00092223
Volume
43
Issue
4
Year of publication
1998
Pages
711 - 718
Database
ISI
SICI code
0009-2223(1998)43:4<711:AOTFDO>2.0.ZU;2-M
Abstract
Modern TLC equipment was used for quantitative determination of high e xplosives residues in soil and water. Chromatograms were developed in reversed-phase system by automated multiple development gradient eluti on. Analytes were extracted from matrix using liquid-liquid extraction (LLE) and solid phase extraction techniques. The recoveries (for soil and water they were 70-80 % and 90-98 % respectively) and detectabili ty limits (50-200 ng in band) were estimated. Quantitation was carried out by UV or VIS absorption light measurement in situ.