LIQUID-CHROMATOGRAPHIC SEPARATION OF INTERMEDIATES OF THE CATALYTIC-HYDROGENATION OF 2,4-DINITROTOLUENE

Authors
MUSOLINO MG NERI G MILONE C MINICO S GALVAGNO S
Citation
Mg. Musolino et al., LIQUID-CHROMATOGRAPHIC SEPARATION OF INTERMEDIATES OF THE CATALYTIC-HYDROGENATION OF 2,4-DINITROTOLUENE, Journal of chromatography, 818(1), 1998, pp. 123-126
Citations number
8
Categorie Soggetti
Chemistry Analytical","Biochemical Research Methods
Journal title
Journal of chromatography → ACNP
Volume
818
Issue
1
Year of publication
1998
Pages
123 - 126
Database
ISI
SICI code
Abstract
An improved HPLC method was developed for the separation and quantific ation of 2,4-dinitrotoluene and its reduction products. Gradient eluti on, with a water-acetonitrile mobile phase, was selected for the separ ation of ail components including the 2,4-nitrohydroxyaminotoluene iso mers. Provisional identification of the isomer intermediates has been obtained by their UV-Vis spectra. (C) 1998 Elsevier Science B.V. All r ights reserved.