SYNTHESIS AND CHARACTERIZATION OF TITANIUM(IV) COMPLEXES OF BENZYLMONOTHIOSEMICARBAZONE

Citation
Ms. Singh et al., SYNTHESIS AND CHARACTERIZATION OF TITANIUM(IV) COMPLEXES OF BENZYLMONOTHIOSEMICARBAZONE, Phosphorus, sulfur and silicon and the related elements, 130, 1997, pp. 107-113
Citations number
18
ISSN journal
10426507
Volume
130
Year of publication
1997
Pages
107 - 113
Database
ISI
SICI code
1042-6507(1997)130:<107:SACOTC>2.0.ZU;2-F
Abstract
Titanium(TV) derivatives of benzilmonothiosemicarbazone have been synt hesised by the reaction of titanium tetrachloride with the sodium salt of benzilmonothiosemicarbazone (prepared in situ) in 1: 1, 1:2, 1:3 a nd 1:4 molar ratios and have been characterised on the basis of elemen tal (C, H, N, S, Cl and Ti) analyses, molecular weight determinations and spectral (IR and PMR) studies.