Ms. Singh et al., SYNTHESIS AND CHARACTERIZATION OF TITANIUM(IV) COMPLEXES OF BENZYLMONOTHIOSEMICARBAZONE, Phosphorus, sulfur and silicon and the related elements, 130, 1997, pp. 107-113
Titanium(TV) derivatives of benzilmonothiosemicarbazone have been synt
hesised by the reaction of titanium tetrachloride with the sodium salt
of benzilmonothiosemicarbazone (prepared in situ) in 1: 1, 1:2, 1:3 a
nd 1:4 molar ratios and have been characterised on the basis of elemen
tal (C, H, N, S, Cl and Ti) analyses, molecular weight determinations
and spectral (IR and PMR) studies.