H. Fujiwara et al., CRYSTALLOGRAPHIC ANALYSIS OF THE RELATIONSHIP BETWEEN BCC AND HCP PHASES IN TITANIUM-ALLOYS BY KIKUCHI PATTERNS, Nippon Kinzoku Gakkaishi, 62(9), 1998, pp. 803-811
Crystallography of ol(HCP) phase precipitated in beta (BCC) grains of
a Ti-22 mass%V-4 mass%Al alloy has been studied using the Kikuchi patt
erns obtained by transmission electron microscopy. The relative orient
ation relationship between or precipitates and beta matrix grains was
determined by an analysis of the Kikuchi patterns taken from HCP and B
CC phases. The analytical error was evaluated by the study of {1 (1) o
ver bar 01}(hcp) transformation twins in the martensite phase formed i
n a rapidly quenched commercially pure titanium specimen. Comparison o
f the experimental results obtained from the twins with the theoretica
l calculation has shown that the rotation angular error was less than
0.10 degrees. The orientation relationship of intragranular ct precipi
tates have a slight deviation from the exact Burgers orientation relat
ionship. The average deviation angle was 0.68 degrees for the parallel
plane relationship, ie., (0001)(alpha)/(110)(beta), and 0.61 degrees
for the parallel direction relationship, i.e., [2 (1) over bar (1) ove
r bar 0](alpha)/[1 (1) over bar 1](beta). The grain boundary a precipi
tates were found to have the Potter orientation relationship rather th
an the Burgers orientation relationship with one of the adjacent beta
grains.