Semiconductor nanoparticles were synthesized by exposing fatty acid sa
lt Langmuir-Blodgell films to the atmosphere of H2S. The particle size
s were characterized by small-angle x-ray scattering of their solution
s using synchrotron radiation source at higher resolution, as it was i
mpossible previously to study it with usual laboratory x-ray sources.
The particle sizes were found to correspond with the demands of single
-electron and quantum junctions. Semiconductor heterostructures were g
rown by self-aggregation of these particles of different types. Electr
ical properties of these nanostructures were studied by using STM. Vol
tage-current characteristics revealed the presence of differential neg
ative resistance. Measurements confirmed the formation of semiconducto
r superlattices directed towards a development of new nanodevices, suc
h as tunnelling diodes and semiconductor lasers.