Thermograms are curves resulting from thermal analysis and are of great int
erest in the study of various food and biological products physical propert
ies. A method to separate underlying peaks is proposed, and statistical pro
perties of estimates for some characteristic parameters are derived. The to
tal number of peaks can be estimated with a sequential analysis of the resi
dual plots. For each new peak, a statistical criterion is proposed to check
whether it is significantly different from the noise of the recording. As
an example, the method is applied to it summer milk fat fusion thermogram.