RELATION BETWEEN INTERNAL BOUNDARIES AND CRITICAL-CURRENT IN TEXTUREDYBA2CU3O7-DELTA - TRANSMISSION ELECTRON-MICROSCOPE OBSERVATIONS

Citation
A. Khalfi et al., RELATION BETWEEN INTERNAL BOUNDARIES AND CRITICAL-CURRENT IN TEXTUREDYBA2CU3O7-DELTA - TRANSMISSION ELECTRON-MICROSCOPE OBSERVATIONS, Journal of materials research, 13(10), 1998, pp. 2800-2806
Citations number
21
Categorie Soggetti
Material Science
ISSN journal
08842914
Volume
13
Issue
10
Year of publication
1998
Pages
2800 - 2806
Database
ISI
SICI code
0884-2914(1998)13:10<2800:RBIBAC>2.0.ZU;2-H
Abstract
The local critical current (I-c) at 77 K measured at the mm scale in a 60 mm long sample of YBa2Cu3O7-delta prepared by a melting zone proce ss is correlated to the microstructure. Lower values of I-c (<20 A) we re obtained in a part of the sample which optical microscope examinati on showed to be generally polycrystalline. In contrast, the rest of th e sample, consisting mostly of large textured domains, gave values for I-c of 120 A and above. Transmission electron microscope observations revealed that the textured domains contain internal boundaries. Depen ding on the scale of observation, the misorientation angles across the boundaries could vary from a few tenths of a degree up to a few degre es. This seems characteristic for boundaries in textured material whic h allow strong coupling of the superconducting current across themselv es.