A. Khalfi et al., RELATION BETWEEN INTERNAL BOUNDARIES AND CRITICAL-CURRENT IN TEXTUREDYBA2CU3O7-DELTA - TRANSMISSION ELECTRON-MICROSCOPE OBSERVATIONS, Journal of materials research, 13(10), 1998, pp. 2800-2806
The local critical current (I-c) at 77 K measured at the mm scale in a
60 mm long sample of YBa2Cu3O7-delta prepared by a melting zone proce
ss is correlated to the microstructure. Lower values of I-c (<20 A) we
re obtained in a part of the sample which optical microscope examinati
on showed to be generally polycrystalline. In contrast, the rest of th
e sample, consisting mostly of large textured domains, gave values for
I-c of 120 A and above. Transmission electron microscope observations
revealed that the textured domains contain internal boundaries. Depen
ding on the scale of observation, the misorientation angles across the
boundaries could vary from a few tenths of a degree up to a few degre
es. This seems characteristic for boundaries in textured material whic
h allow strong coupling of the superconducting current across themselv
es.