SYNTHESIS AND CRYSTAL-STRUCTURE OF A NOVEL GERMATRANE - 1-BIS(TRIMETHYLSILYL) AMINOGERMATRANE

Citation
Sn. Nikolaeva et al., SYNTHESIS AND CRYSTAL-STRUCTURE OF A NOVEL GERMATRANE - 1-BIS(TRIMETHYLSILYL) AMINOGERMATRANE, Zeitschrift fur Naturforschung. B, A journal of chemical sciences, 53(9), 1998, pp. 973-976
Citations number
22
Categorie Soggetti
Chemistry Inorganic & Nuclear","Chemistry Inorganic & Nuclear
ISSN journal
09320776
Volume
53
Issue
9
Year of publication
1998
Pages
973 - 976
Database
ISI
SICI code
0932-0776(1998)53:9<973:SACOAN>2.0.ZU;2-N
Abstract
1-Bis(trimethylsilyl)aminogermatrane (3), the first germatrane bearing an amino group at the germanium atom, was synthesized by the reaction of 1-hydroxygermatrane with bis[bis(trimethylsilyl)amino)]stannylene (1). 3 has been characterised by H-1,C-13, Si-29 NMR spectroscopy, ele mental analysis, and by X-ray diffractometry.