Gj. Shen et al., TWIN FORMATION DUE TO IRRADIATION OF ENERGETIC ELECTRON-BEAM IN HIGH-TEMPERATURE SUPERCONDUCTORS OF IN-DOPED AND SB-DOPED YBCO, Physica. C, Superconductivity, 214(3-4), 1993, pp. 426-434
Twins and twin boundaries existing in the YBCO and In- and Sb-doped YB
CO high-T(c) ceramic superconductors were observed by means of a trans
mission electron microscope. The orientation of the twins was determin
ed from the electron diffraction pattern using the operation voltage o
f 160 kV. By the conventional extinction method the image of twins cou
ld be revealed with a better contrast, so that they might be observed
more clearly. Based on the TEM observation, we have proposed a model f
or twin formation in the perovskite structure. The energy for twin bou
ndary formation has also been roughly estimated to be 44.0 mJ/m2.