1ST OBSERVATION OF BULK MAGNETIC SCATTERING USING HIGH-ENERGY X-RAYS

Citation
T. Bruckel et al., 1ST OBSERVATION OF BULK MAGNETIC SCATTERING USING HIGH-ENERGY X-RAYS, Acta crystallographica. Section A, Foundations of crystallography, 49, 1993, pp. 679-682
Citations number
14
Categorie Soggetti
Crystallography
ISSN journal
01087673
Volume
49
Year of publication
1993
Part
4
Pages
679 - 682
Database
ISI
SICI code
0108-7673(1993)49:<679:1OOBMS>2.0.ZU;2-3
Abstract
Today, the most powerful methods for the investigation of magnetic str uctures are magnetic neutron diffraction and synchrotron-X-ray scatter ing in the energy range 3 - 15 keV. This paper reports the first succe ssful experiment to exploit a new technique: the magnetic diffraction of hard X-rays with energies exceeding 80 keV. This technique combines some of the advantages of each of the aforementioned methods: namely high Q-space resolution (10(-4) angstrom-1 radial and 10(-5) angstrom- 1 tangential) and bulk sensitivity (absorption length >> 1 mm). It is shown that, compared to nominally 10 keV X-ray scattering, enhancement factors of several orders of magnitude can be obtained for the magnet ic signal, owing to the increase in penetration depth. The magnetic cr oss section for these very hard X-rays is discussed, the new technique is compared with the existing methods and a preliminary experiment on MnF2 is reported.