M. Ullrich et al., CRITICAL CURRENTS AND MICROSTRUCTURE OF MELT-TEXTURED STOICHIOMETRIC YBA2CU3O7-DELTA CRYSTALLITES, Physical review. B, Condensed matter, 48(10), 1993, pp. 7513-7517
To avoid weak-link behavior caused by grain boundaries small crystalli
tes of YBa2Cu3O7-delta were mechanically separated from approximately
1 cm3 Bridgman-melt-textured blocks. Using the Bean critical-state mod
el, j(c) values at 4 K and 5 T (70 K and 2 T) as high as approximately
2 X 10(6) A/cm2 (approximately 4 X 10(4) A/cm2) were estimated from t
he width of the magnetization hysteresis. Microstructural investigatio
ns of the crystallites reveal the existence of dislocations, finely di
stributed inclusions, stacking faults, twin boundaries, elementary gro
wth steps, and oxygen-deficient regions. The defects are thought to ha
ve a strong influence on the pinning behavior and the shape of the mag
netization curve.