A. Siwek et al., SINTERING PROCESS AND MECHANICAL-PROPERTIES IN STEEL SUPERCONDUCTOR GRANULAR COMPOSITES/, Solid state ionics, 112(1-2), 1998, pp. 79-85
A study of two-phase composite pellets obtained from powders of stainl
ess steel and of a bismuth cuprate superconductor (Bi2-xPbxSr2Ca2Cu3O1
0-x) has been carried out, using scanning electron microscopy, magneti
c field expulsion analyses and elastic modulus measurements. Each comp
osite sample is defined by its initial volume fraction, its sintering
temperature and sintering duration. The magnetic responses of the comp
osites are determined from levitation experiments. The Young modulus E
and the elastic limit R-c are measured from compression experiments.
A correlation between the scanning electron images, the levitation for
ces F-lev and the elastic properties is established. When the volume f
raction of steel or the sintering temperature increase, the Young modu
lus E and the elastic limit R-c both decrease. When the sintering dura
tion increases, the elastic properties are improved. The role of pores
and of the liquid phase formed during the sintering process is discus
sed. (C) 1998 Elsevier Science B.V. All rights reserved.