P. Baruah et Jcs. Kataky, PHOSPHORUS-HETEROCYCLES - PART 2 - SYNTHESIS OF DELTA(5)-1,2,3-DIAZAPHOSPHOLINES AND DELTA(5)-1,2,3-AZAOXAPHOSPHOLINES FROM HYDRAZONES AND OXIMES, Indian Journal of Heterocyclic Chemistry, 8(1), 1998, pp. 43-46
The phenylhydrazones (2-4) and oximes (8) of acetophenone and substitu
ted acetophenones react with phenyl)-1,3,2,4-dithiadiphosphetane-2,4-d
isulphide (Lawesson's reagent) (i) to give Delta(5)-1,2,3-diazaphospho
lines (5-7) and Delta(5)-1,2,3-azaoxaphospholines (9). The structures
of the compounds were confirmed with the help of physical and spectral
data.