E. Ramos et al., OBTENTION OF A BREWED COFFEE AROMA EXTRACT BY AN OPTIMIZED SUPERCRITICAL CO2-BASED PROCESS, Journal of agricultural and food chemistry, 46(10), 1998, pp. 4011-4016
Supercritical fluid extraction (SFE) was used to obtain brewed coffee
extracts with an aroma as similar as possible to the original brewed c
offee. The optimization of the process operating variables was perform
ed by means of a sequential simplex method whose response was based on
the sensorial evaluation of the aroma extracts. Subsequently, the com
position of the extracts obtained at the optimal SFE conditions was de
termined by using a purge-and-trap device coupled to a GC-MS. For comp
arison, extracts obtained by using liquid - liquid extraction and head
space-solid-phase microextraction were also obtained and analyzed by G
C-MS.