This paper presents the main results of a study about a new method for
drying organic resorcinol-formaldehyde gels: freeze-drying. The obtai
ned material has a good cohesion and presents an important porous volu
me (up to 9.5 cm(3)/g) and a large specific surface area (up to 300 m(
2)/g). It is shown that the drying operating conditions and particular
ly the freezing rate and the surface/volume ratio of the gel samples m
odify the textural characteristics of the aerogel.