DETERMINATION OF NAPHTHALENESULPHONATES IN WATER BY ONLINE ION-PAIR SOLID-PHASE EXTRACTION AND ION-PAIR LIQUID-CHROMATOGRAPHY WITH DIODE-ARRAY UV DETECTION

Authors
ELHARRAK R CALULL M MARCE RM BORRULL F
Citation
R. Elharrak et al., DETERMINATION OF NAPHTHALENESULPHONATES IN WATER BY ONLINE ION-PAIR SOLID-PHASE EXTRACTION AND ION-PAIR LIQUID-CHROMATOGRAPHY WITH DIODE-ARRAY UV DETECTION, International journal of environmental analytical chemistry (Print), 69(4), 1998, pp. 295-305
Citations number
12
Categorie Soggetti
Environmental Sciences","Chemistry Analytical
Journal title
International journal of environmental analytical chemistry (Print) → ACNP
ISSN journal
03067319
Volume
69
Issue
4
Year of publication
1998
Pages
295 - 305
Database
ISI
SICI code
0306-7319(1998)69:4<295:DONIWB>2.0.ZU;2-J
Abstract
Ion-pair solid-phase extraction was on-line coupled to a chromatograph ic system with a PLRP-s precolumn and the results were compared with t hose obtained when C-18 sorbents are used. After optimization, the met hod was used to determine these compounds in two river waters. A sampl e of 20 ml of river water was preconcentrated with good recovery value s for all the compounds studied and detected at 220 nm with detection limits between 0.25 and 0.1 mu g l(-1). Some of the compounds were pro visionally determined by diode-array UV detection.