CONDUCTION CALORIMETERS - HEAT TRANSMISSION-SYSTEMS WITH UNCERTAINTIES

Citation
V. Torra et H. Tachoire, CONDUCTION CALORIMETERS - HEAT TRANSMISSION-SYSTEMS WITH UNCERTAINTIES, JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 52(3), 1998, pp. 663-681
Citations number
47
Categorie Soggetti
Chemistry Analytical","Chemistry Physical
Journal title
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
ISSN journal
13886150 → ACNP
Volume
52
Issue
3
Year of publication
1998
Pages
663 - 681
Database
ISI
SICI code
0368-4466(1998)52:3<663:CC-HTW>2.0.ZU;2-P
Abstract
A critical reading of early papers on heat flux or conduction calorime try (1920-1965) reveals the original kinetic aims of the developed ins trumentation and the progressive appearance of the intrinsic difficult ies. An analysis of current publications demonstrates biased applicati ons/results relating to equivalent problems. Modelling of the systems by the RC analogy of heat transfer equations establishes the problems connected with the structure of the apparatus and also the experimenta l conditions to be fulfilled. Analysis of the equations highlights sev eral possibilities that are used in part today. For instance, the redu ction of noise and drift on the calorimeter output by a software appro ach and the conditions to be attained with crucibles for increased acc uracy.