M. Hoummady et E. Farnault, ENHANCED SENSITIVITY TO FORCE GRADIENTS BY USING HIGHER FLEXURAL MODES OF THE ATOMIC-FORCE MICROSCOPE CANTILEVER, Applied physics A: Materials science & processing, 66, 1998, pp. 361-364
Higher flexural modes of a Si cantilever are used in order to increase
the operating frequencies in non-contact mode scanning force microsco
py. By recording frequency responses at different tip-sample distances
and by using different flexural modes, long-range tip-sample interact
ions are studied. The experimental results reveal that operating at hi
gher resonant modes makes it possible to improve sensitivity to force
gradients and to avoid overlap between hydrodynamic interactions and a
ttractive interactions in the range of 100-nm tip-sample distances. Us
ing the second-harmonic, a sevenfold-enhanced sensitivity is demonstra
ted. Finally, discussion on the appropriate technique related to force
gradient measurement, i.e. slope detection or frequency modulation te
chnique, is reported.