M. Kempf et al., NANOHARDNESS MEASUREMENTS FOR STUDYING LOCAL MECHANICAL-PROPERTIES OFMETALS, Applied physics A: Materials science & processing, 66, 1998, pp. 843-846
Studying local mechanical properties of metallic alloys and composites
and their defect structures such as grain boundaries, cracks, and dis
locations allows a better understanding and design of these structural
materials. With a nanoindenting atomic force microscope (NI-AFM), whi
ch uses diamond tips, such measurements are possible on a nanometer sc
ale. Measurements on the microstructure of superalloys are presented,
where different precipitates with sizes in the range of 100 nm are cha
racterized by their different hardness values. In addition, this new t
echnique was used to characterize the nanohardness of the plastic zone
and stress fields of cracks and grain boundaries. Therefore, crack ti
ps of in-situ loaded bending specimens of intermetallic alloys (NiAl)
were investigated. The measurements show a change in nanohardness and
elasticity from the distance of interfaces.