Jb. Benziger et al., A SCINTILLATOR PURIFICATION SYSTEM FOR A LARGE-SCALE SOLAR-NEUTRINO EXPERIMENT, Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment, 417(2-3), 1998, pp. 278-296
An on-line purification system for a large-scale low-background liquid
scintillation detector has been tested with the 5 t liquid scintillat
ion detector, the Counting Test Facility at Gran Sasso. Counter-curren
t water extraction removes polar and charged impurities such as ions a
nd metal salts. Vacuum distillation of the entire scintillator has bee
n applied to remove both radioactive impurities and chemical impuritie
s that affect the optical properties of the scintillator. Filtration w
ith a 0.05 mu m particulate filter removed suspended dust particles th
at may contain U, Th and K, Nitrogen stripping was employed to remove
dissolved water and noble gases (e.g. Kr-85) from the scintillator. Th
e system has effectively reduced the internal back in the 5 t liquid s
cintillation detector from 470 +/- 90 events/d to the detection limit
of the detector (+/- 45 events/d) in the energy window 250 < E < 800 k
eV. (C) 1998 Elsevier Science B.V. All rights reserved.