The formation of copper microcrystallites on a Cu/Fe/Cu(100) sandwich
due to annealing at temperatures between 500 K and 600 K was studied.
For the crystallites to form, the iron film thickness must be more tha
n 10 monolayers (bcc-Fe) and the copper film thickness must be in the
range of 3-10 monolayers. The formation process of the crystallites wa
s investigated using a newly developed apparatus allowing scanning ele
ctron, scanning Auger and scanning tunneling microscopy on the same sa
mple position and repeated repositioning to a given position. The crys
tallites were found to form mainly at step bunches and predominantly o
riented along the [110] directions of the copper substrate. A large nu
mber of screw dislocations are visible on top of the crystallites. The
growth of the crystallites was observed by sequential measuring/annea
ling cycles. The results are discussed in terms of the structural tran
sformation of the Cu/Fe/Cu sandwich.