High-resolution SIMS images in conjunction with elastically backscatte
red electron and energy-dispersive x-ray images have been acquired fro
m a polished slightly oxidized multiphase polycrystalline surface of N
i-Cu sulphide ore. Through correlation of data acquired by the three m
ethods, the extent to which oxidation occurs is shown to be mineral de
pendent and related to the presence of macroscopic and microscopic sur
face heterogeneities. (C) 1998 John Wiley & Sons, Ltd.