TOWARDS 0.1 NM RESOLUTION WITH THE FIRST SPHERICALLY CORRECTED TRANSMISSION ELECTRON-MICROSCOPE

Citation
M. Haider et al., TOWARDS 0.1 NM RESOLUTION WITH THE FIRST SPHERICALLY CORRECTED TRANSMISSION ELECTRON-MICROSCOPE, Journal of Electron Microscopy, 47(5), 1998, pp. 395-405
Citations number
31
Categorie Soggetti
Microscopy
ISSN journal
00220744
Volume
47
Issue
5
Year of publication
1998
Pages
395 - 405
Database
ISI
SICI code
0022-0744(1998)47:5<395:T0NRWT>2.0.ZU;2-W
Abstract
A hexapole corrector which compensates for the spherical aberration of the objective lens has been incorporated in a commercial 200 kV trans mission electron microscope (TEM) equipped with a field emission gun. The successful correction of the spherical aberration is demonstrated by decreasing the instrumental resolution limit from 0.24 nm down to a bout 0.13 nm. Images of Si-SiCO2 interfaces obtained with the correcte d TEM show a remarkable suppression of artefacts and a strong increase in contrast apart from the improved resolution. The design, alignment and the performance of the corrected instrument are outlined in detai l.