PREPARATION AND MECHANISM OF FORMATION OF ACICULAR GOETHITE-MAGNETITEPARTICLES BY DECOMPOSITION OF FERRIC AND FERROUS SALTS IN AQUEOUS-SOLUTION USING MICROWAVE-RADIATION
Gh. Wang et al., PREPARATION AND MECHANISM OF FORMATION OF ACICULAR GOETHITE-MAGNETITEPARTICLES BY DECOMPOSITION OF FERRIC AND FERROUS SALTS IN AQUEOUS-SOLUTION USING MICROWAVE-RADIATION, Materials research bulletin, 33(11), 1998, pp. 1571-1579
Acicular geothite-magnetite particles were prepared directly by microw
ave-driven hydrolysis of an aqueous solution of ferric and ferrous sal
ts in the ratio Fe3+:Fe2+ = 1:2, which is appropriate to magnetite. Th
e experimental conditions that influence the shape and size of the par
ticles were determined, and the mechanism of the formation of acicular
particles is discussed. (C) 1998 Elsevier Science Ltd.