By redshift z = 10, star formation in the first objects should have produce
d considerable amounts of carbon, nitrogen, and oxygen. The submillimeter l
ines of C, N, and O redshift into the millimeter and centimeter bands (0.5
mm-1.2 cm), where they may be detectable. High spectral resolution observat
ions could potentially detect inhomogeneities in C, N, and O emission, and
see the first objects forming at high redshift. We calculate expected inten
sity fluctuations and discuss frequency and angular resolution required to
detect them. For C II emission, we estimate the intensity using two indepen
dent methods: the line-emission coefficient argument and the luminosity-den
sity argument. We find they are in good agreement. At 1 + z similar to 10,
the typical protogalaxy has a velocity dispersion of 30 km s(-1) and an ang
ular size of 1 ". If C II is the dominant coolant, then we estimate a chara
cteristic line strength of similar to 0.1 K km s(-1) We also discuss other
atomic lines and estimate their signal. Observations with a frequency resol
ution of 10(-3) can detect moderately nonlinear fluctuations of amplitude 2
x 10(-5) times the microwave background. If the intensity fluctuations are
detected, they will probe matter density inhomogeneity, chemical evolution
, and ionization history at high redshifts.