SYNTHESIS OF [H-2(11)]CYCLOHEXANOL BY REDUCTION OF PENTACHLOROPHENOL USING RANEY NICKEL-ALUMINUM ALLOY IN A BAO-D-2,O SOLUTION UNDER SONICATION

Authors
MUKUMOTO M MASHIMO T TSUZUKI H TSUKINOKI T UEZU N MATAKA S TASHIRO M KAKINAMI T
Citation
M. Mukumoto et al., SYNTHESIS OF [H-2(11)]CYCLOHEXANOL BY REDUCTION OF PENTACHLOROPHENOL USING RANEY NICKEL-ALUMINUM ALLOY IN A BAO-D-2,O SOLUTION UNDER SONICATION, Journal of chemical research. Synopses, (10), 1995, pp. 412-413
Citations number
8
Categorie Soggetti
Chemistry
Journal title
Journal of chemical research. Synopses → ACNP
ISSN journal
03082342
Issue
10
Year of publication
1995
Pages
412 - 413
Database
ISI
SICI code
0308-2342(1995):10<412:SO[BRO>2.0.ZU;2-4
Abstract
Reduction of pentachlorophenol (1) with Raney nickel-aluminium alloy i n saturated BaO-D2O under sonication afforded [2H(11)]cyclohexanol (2) in 85% yield with a high [H-2]-content (99%).