Thirty-two batches of semi-hard cheese containing ca. 46% fat in dry matter
were produced in a pilot plant in an experimental design with pH, moisture
and microbiological contamination with Clostridium tyrobutyricum and propi
onibacteria as controlled variables. The cheeses were measured ungrated aft
er 5, 7, 9 and 11 weeks of ripening by near infrared (NIR) spectroscopy in
transmittance mode (850-1050 nm) and in reflectance mode (1110-2490 nm). Se
nsory properties were evaluated by a panel of 10 assessors. Calibration equ
ations were developed by partial least-squares (PLS) regression on consiste
ncy and flavour attributes. Generally, the accuracy of near-infrared reflec
tance spectroscopy was better than that of transmittance spectroscopy. The
squared correlation coefficients (R-2) obtained by NIR reflectance spectros
copy were 0.74-0.88 for consistency attributes and 0.27-0.59 for flavour at
tributes. Depending on the attribute, the standard error of prediction corr
esponded to the standard error of reproducibility of the average score from
2 to 6 assessors. (C) 1999 Elsevier Science Ltd. All rights reserved.