S. Kramer et J. Mayer, Using the Hough transform for HOLZ line identification in convergent beam electron diffraction, J MICROSC O, 194, 1999, pp. 2-11
The Hough transform as a means for automatic line detection is applied for
higher order Laue zone (HOLZ) line identification in convergent beam electr
on diffraction, The HOLZ line positions are commonly used to measure the st
rain state in the investigated material. Besides the automation, a very imp
ortant aspect is the accuracy of the detected line positions. The limits ar
e determined by the amount of noise in the pattern relative to the contrast
of the HOLZ lints and the line width. Our investigations show that sub-pix
el resolution can be achieved routinely. We have also developed a new strai
n analysis procedure in which the dynamical shift of each individual line c
an be taken into account using a model based on several Ewald spheres with
different radii, In comparison to the effective high voltage method, finer
details of the dispersion surface can be considered, which increases the ac
curacy of the strain analysis. A measurement of the thermal expansion of al
uminium is presented as a model experiment, The lattice constants were dete
rmined with an accuracy of about 10(-4).