INFLUENCE OF HETEROGENEOUS DISLOCATION ARRANGEMENTS ON X-RAY-DIFFRACTION PROFILES MEASURED ON CYCLICALLY DEFORMED NICKEL SINGLE-CRYSTALS .1. PROFILE BROADENING AT DIFFERENT PLASTIC STRAIN AMPLITUDES
M. Hecker et al., INFLUENCE OF HETEROGENEOUS DISLOCATION ARRANGEMENTS ON X-RAY-DIFFRACTION PROFILES MEASURED ON CYCLICALLY DEFORMED NICKEL SINGLE-CRYSTALS .1. PROFILE BROADENING AT DIFFERENT PLASTIC STRAIN AMPLITUDES, Zeitschrift fur Metallkunde, 88(4), 1997, pp. 321-328
X-ray diffraction profiles of Bragg reflections were measured on cycli
cally deformed nickel single crystals of different orientations with a
high-resolution double crystal diffractometer. The mesoscopic disloca
tion structures beneath the crystal surfaces were studied by scanning
electron microscopy using the channelling contrast of backscattered el
ectrons. Changes of internal stresses on different length scales can b
e inferred from the characteristic dependence of the diffraction profi
le broadening on the plastic strain amplitude. Short-range stresses ar
e predominant in the matrix structure of crystals cyclically deformed
at small strain amplitudes. At higher amplitudes, in the plateau regio
n of the cyclic stress-strain curve, remarkable long-range stresses ar
ise in crystals of all orientations due to the existence of ladder-lik
e, cellular and other dislocation structures.