Sh. Lee et al., Effects of binder and thermal debinding parameters on residual carbon in injection moulding of Nd(Fe,Co)B powder, POWD METALL, 42(1), 1999, pp. 41-44
Thermal debinding properties of several organic binders for the injection m
oulding of Nd(Fe,Co)B powder have been investigated. The investigation incl
uded analysis of the residual carbon content, which affects the magnetic pr
operties of the sintered magnet. The effect of several debinding parameters
such as specimen thickness, debinding atmosphere, gas flowrate, heating ra
te, and debinding temperature were also studied. Depending on the pyrolysis
mechanism, binders gave specific results for the residual carbon. The mole
cular weight was found to have a large effect on the residual carbon and sh
owed a logarithmic linear increase with increase in residual carbon. Hydrog
en gas was found to be the most appropriate atmosphere for the debinding of
the moulded specimens. Slow heating and high temperature were found to be
effective for low residual carbon. Gas flowrate showed little effect and sp
ecimen thickness showed no effect, except with stearic acid.