Selective 1D H-1 -> C-13 -> C-13 polarization transfer experiments for small organic molecules

Citation
L. Poppe et al., Selective 1D H-1 -> C-13 -> C-13 polarization transfer experiments for small organic molecules, MAGN RES CH, 37(5), 1999, pp. 382-384
Citations number
19
Categorie Soggetti
Spectroscopy /Instrumentation/Analytical Sciences
Journal title
MAGNETIC RESONANCE IN CHEMISTRY
ISSN journal
07491581 → ACNP
Volume
37
Issue
5
Year of publication
1999
Pages
382 - 384
Database
ISI
SICI code
0749-1581(199905)37:5<382:S1H-C->2.0.ZU;2-J
Abstract
Selective polarization transfer from proton to adjacent carbon was accompli shed by either selective cross-polarization or selective refocused-INEPT. M agnetization was transferred in the subsequent step to remote carbons separ ated by one, two or three bonds. The acquired data were processed by a new symmetrization protocol resulting in the signal-to-noise ratio enhancement by a factor of root 2. Copyright (C) 1999 John Wiley & Sons, Ltd.