Oxides that were grown on Zr-20Nb in water at 300 degrees C for 3 d, or in
air at 400 degrees C for less than or equal to 2 h were characterized by an
alytical electron microscopy. In both oxides. a similar microstructure was
observed and similar electron diffraction patterns and high resolution latt
ice images were obtained. Analyses of the results showed that the crystal s
tructure of the oxides was identical to that of an incommensurate modulated
Nb2Zrx-2O2x+1 phase, with x approximate to 10. (C) 1999 Published by Elsev
ier Science B.V. All rights reserved.