H. Rameback et M. Skalberg, A separation procedure for the analysis of Sr-90, Eu-154, and the actinides Np-237, Pu-239, Am-241 and Cm-244, J RAD NUCL, 240(2), 1999, pp. 661-663
A procedure for the analysis of Sr-90, Eu-154, Np-237, Pu-239, Am-241 and C
m242-244 was developed. Separation was done with the separating agent, di-2
(ethyl hexyl)-phosphoric acid (HDEHP), and results in fractions containing
the different elements to be analysed. 90Sr analysis was done by analysing
its daughter nuclide Y-90, detected through the Cherenkov radiation emitted
by this high energy beta(-)-emitter. Eu-154 was detected using gamma-spect
rometry with a lower Compton background as a result of the removal of other
fission products. Am-241 could also be detected with gamma-spectrometry or
together with Cm242-244 With alpha-spectrometry. The long-lived radionucli
des Np-237 and Pu-239 were detected using inductively coupled plasma mass s
pectrometry (ICP-MS).