The change of the structure by mechanical alloying on the Fe73.5Cu1Nb3
Si13.5B9 nanostructured alloy was studied experimentally. It was found
that the nanostructured ribbons obtained from the crystallization of
amorphous state by a proper annealing treatment can be changed into am
orphous powder via short time milling. By increasing the milling time,
the milled powder returns to crystallization and exhibits smaller cry
stal size. A still smaller crystal size can be formed if the milled po
wder is annealed again. (C) 1997 Acta Metallurgica Inc.