P. Donnadieu et al., A quantitative study by transmission electron microscopy of nanoscale precipitates in Al-Mg-Si alloys, PHIL MAG A, 79(6), 1999, pp. 1347-1366
We report a quantitative study of hardening precipitates carried out by mea
ns of transmission electron microscopy (TEM). Several TEM techniques are co
upled to draw quantitative information without the help of a hypothesis on
the precipitate structure and composition. The method is illustrated by an
investigation of hardening precipitates in an Al-Mg-Si alloy 6056 (T6 tempe
r). This microstructure consists of two precipitate families: lath and rod.
The TEM study leads for the rod precipitate to a volume fraction of 1.3 +/
- 0.1% and a number density of 8.6 +/- 0.4 x 10(16) cm(3) We also obtained
the rod size distribution and a mean rod diameter of 2.86 nm. The lath prec
ipitate volume fraction and density are also estimated but with less precis
ion. The present results are discussed in comparison with a previous small-
angle scattering study carried out on the same material.