Wk. Rhim et al., Noncontact technique for measuring surface tension and viscosity of moltenmaterials using high temperature electrostatic levitation, REV SCI INS, 70(6), 1999, pp. 2796-2801
A new, noncontact technique is described which entails simultaneous measure
ments of the surface tension and the dynamic viscosity of molten materials.
In this technique, four steps were performed to achieve the results: (1) a
small sample of material was levitated and melted in a high vacuum using a
high temperature electrostatic levitator, (2) the resonant oscillation of
the drop was induced by applying a low level ac electric field pulse at the
drop of resonance frequency, (3) the transient signals which followed the
pulses were recorded, and (4) both the surface tension and the viscosity we
re extracted from the signal. The validity of this technique was demonstrat
ed using a molten tin and a zirconium sample. In zirconium, the measurement
s could be extended to undercooled states by as much as 300 K. This techniq
ue may be used for both molten metallic alloys and semiconductors. (C) 1999
American Institute of Physics. [S0034-6748(99)00206-3].