Jt. Cardin et al., Quasioptical design for an EPR spectrometer based on a horizontal-bore superconducting solenoid, APPL MAGN R, 16(2), 1999, pp. 273-292
We describe a novel high-frequency electron paramagnetic resonance (HF-EPR)
spectrometer design based on a horizontal-bore superconducting solenoid. D
esigns for components of a quasioptical HF-EPR spectrometer operating with
a horizontal-bore 7.85 T solenoid are discussed. A rigid concentric tube co
nstruction permits precise placement and control of the optical elements in
the magnet bore. A mechanically coupled, sliding optical table bearing the
quasioptical bridge is another essential feature of the design. The horizo
ntal configuration greatly improves optical alignment as well as physical a
ccess to the sample area compared to existing vertical-bore instruments. As
a result, the minimum spin concentration that is detectable with an inexpe
nsive room-temperature diode is comparable to the lowest values reported fo
r aqueous samples in vertical-bore magnets using high-sensitivity detectors
.