SYNTHESIS OF K-ZR PHOSPHATES BY THE MOLTEN-SALT METHOD

Authors
BARABANOVA AV AFANASEV PV KOSTYUK BG LUNIN VV
Citation
Av. Barabanova et al., SYNTHESIS OF K-ZR PHOSPHATES BY THE MOLTEN-SALT METHOD, Russian chemical bulletin, 45(12), 1996, pp. 2698-2702
Citations number
19
Categorie Soggetti
Chemistry
Journal title
Russian chemical bulletin → ACNP
ISSN journal
10665285
Volume
45
Issue
12
Year of publication
1996
Pages
2698 - 2702
Database
ISI
SICI code
1066-5285(1996)45:12<2698:SOKPBT>2.0.ZU;2-H
Abstract
Phosphates of K and Zr of a layered, microporous structure have been o btained by the molten salt method in a potassium nitrate medium in the temperatures ranges 573-823 K. Dependences of the product composition on the P/Zr atomic ratio and the temperature of synthesis were studie d. The substances obtained have been characterized by XRD, H-1 and P-3 1 NMR, and IR spectroscopy, and scanning electron microscopy.