B-Fluorosubstituted cyclopentadienyldicarbollylcobalt and -iron were s
ynthesized. Electrochemical studies of iron eta(5)-C5H5-3,1,2-FeC2B9H1
1-nFn (n = 2-4) complexes were carried out. F-19 NMR, UV, and IR spect
ra of the cobalt and iron complexes were obtained.