We present here a systematic X-ray diffraction study of residual strains in
(1 1 1) Au/Ni multilayers prepared by molecular beam epitaxy on (1 0 0) Cu
substrates deposited on (1 0 0) Si. The measurement of out-of-plane lattic
e spacings allows one to extract the unit cell dimension and, by making som
e assumptions on the strain tensor, to determine the stress and the stress-
fret lattice parameter. A striking difference appears between the two const
ituents of the superlattice, whereas in gold the residual strain appears to
be related to the relaxation of the strain as a function of the layer thic
kness, the nickel parameter is completely controlled by dynamic gold segreg
ation during growth. (C) 1999 Elsevier Science B.V. All rights reserved.