Ors the effect of gap size between baffle outer diameter and tube inner diameter on the mixing characteristics in an oscillatory-baffled column

We report our experimental investigation on the effect of gaps between baff le outer diameter and inner tube diameter on the mixing characteristics, in terms of mixing time and axial dispersion coefficient, in a batch oscillat ory-baffled column. Local concentration profiles are measured using conduct ivity probes at two locations along the height of the column. The mixing ti me was determined based on the equilibrium concentration concept, and the a xial dispersion coefficient was obtained by solving the axial dispersion go verning equation. Comparison of mixing time between the 'push-fit' and 'loo se-fit' baffle arrangements was carried out and the results showed that the existence of a gap of various sizes between the baffle outer and the tube diameters lengthened the time at which the state of uniform mixing is achie ved in such a device. (C) 1999 Society of Chemical Industry.