Citation
Jh. Yu et al., Syntheses of 3,4-O-(1-aryl-1-propylidene)-D-mannitol, SYN COMMUN, 29(15), 1999, pp. 2567-2574
Citations number
11
Categorie Soggetti
Organic Chemistry/Polymer Science
Journal title
SYNTHETIC COMMUNICATIONS
ISSN journal
00397911
→ ACNP
Volume
29
Issue
15
Year of publication
1999
Pages
2567 - 2574
Database
ISI
SICI code
0039-7911(1999)29:15<2567:SO3>2.0.ZU;2-K
Abstract
A new method for selective reaction of 1-aryl-propane-1-ones with 3,4-dihyd
roxy group of D-mannitol in the presence of ZnCl2-BF3. Et2O to 3,4-O-(1-ary
l-1-propylidene)-D-mannitol (C1-C11) is described. The compounds were first
reported and determined by IR, Ms, H-1/C-13 NMR spectra. Among them the st
ructure of C11 was further defined by X-ray diffraction.