This work reports on the study of polyaniline, doped with LiClO4 via pseudo
protonation, by Nuclear Magnetic Resonance and morphology analysis. The Li-
7 NMR spin-lattice relaxation and linewidth investigations were performed f
or two different salt concentrations as a function of the temperature. The
increase of ion concentration strongly affects the relaxation processes. In
formation about electrical conductivity and thermal analysis are also repor
ted.